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    Feasibility Study of Deposition by SUT-PF

    , M.Sc. Thesis Sharif University of Technology Safarzadehamiri, Ali (Author) ; Vosoughi, Naser (Supervisor)
    Abstract
    Sharif University of Technology Plasma Focus (SUT-PF) is a Mather Type DPF device which has a 39 μF capacitor bank with 14 KV charging ability at its ultimate limit corresponding to 7 KJ stored energy. In the first step of this experiment, a test has been done at three distances 5, 7, 10 cm from anode tip with the different number of shots 20, 30, and 40 at 0 constant angles.In the following, a test is done at 5 and 10 degrees with 40 shots, and PF chamber has been filled up with nitrogen gas. Various tests have carried out for survey of this experiment, the result of which are as follow:The X-ray diffraction (XRD) analysis are used in order to reveal if the Nickel or Nickel nitride have... 

    Experimental Study of Mass Ratio and Carbon Nono Tube Size on Impact Toughness in Composite Polymers

    , M.Sc. Thesis Sharif University of Technology Salmani Givi, Foad (Author) ; Hosseini Kordkheili, Ali (Supervisor)
    Abstract
    Nowadays, composites have wide applications in different industries especially in aerospace industry because of their high strength to weight ratio. Epoxy 5052 for its relatively good mechanical properties and high thermal resistance has vaidly use for manufacturing of large composite components. However; fracture toghness of epoxy resins is not good in comparison to their other exceptional properties. Therefore, researchers have endeavored to improve this characteristic with different approaches. One of these methods is nanotechnology. Since the components in aerospace industry are often under impact loads and impact strength of these materials has been less studied, effect of carbon... 

    The Durability of Geopolymer Concrete Confined with Fiber Reinforced Polymer Materials

    , M.Sc. Thesis Sharif University of Technology Anvari Sakhvidi, Mohammad Amin (Author) ; Toufigh, Vahab (Supervisor)
    Abstract
    Material durability is quite critical in corrosive environments. In this study, two hundred and seventy geopolymer concrete specimens with different mix designs were prepared and then wrapped with two different fiber reinforced polymer (FRP) materials. For 12960 hrs (eighteen months), the specimens were exposed to four different pHs (2.5, 7, 7.25, 12.5). The reliability and SEM analysis were performed after modeling the compressive strength over time. Based on the results, the reduction of the compressive strength was up to 22% in an acidic environment. The compressive strength of the specimens was increased up to 11 percent after alkaline solution exposure. The ductility of all specimens... 

    Investigation of Mechanical Properties and Durability of Alkali-activated Slag Concrete Lightened with Scoria and Its Microstructural Study

    , M.Sc. Thesis Sharif University of Technology Mahmoudzadeh Vaziri, Nima (Author) ; Khaloo, Alireza (Supervisor)
    Abstract
    Concrete has long been one of the most widely used materials in the world. Cement, as a major component of concrete, due to the use of fossil fuels in its production process, emitting greenhouse gases such as carbon dioxide, which cause air pollution and environmental issues such as climate change. On the other hand, the wastes of industrial factories such as slag of the Blast furnace, due to their large volume and lack of sufficient space for storage of these wastes, lead to the release of these wastes that have alkaline structures into enviroment, causing environmental pollution Such as embankment pollution. Alkali-activated concrete has prevented the release of these pollutant into the... 

    A Microstructural Investigation on the Influence of Pore Fluid Osmotic Potential on Volume Changes and Soil Water Retention Curve, Low Plasticity Clay

    , M.Sc. Thesis Sharif University of Technology Heydari, Ali (Author) ; Sadeghi, Hamed (Supervisor)
    Abstract
    Understanding many issues related to environmental geotechnics and soil sciences such as: instability and collapse of soil slopes, sinkholes, leakage from landfills and isolation of nuclear landfills, and optimization Agricultural processing depends on our knowledge of the behavior of unsaturated soils and their volume changes. To better understand the behavior of unsaturated soils, it is important to study the soil-water retention curve (SWRC) and the factors affecting it. These include factors such as porosity, grain size distribution, soil minerals, pore size distribution, and pore water chemistry, which affect soil-water retention curves and volume changes. Since the simultaneous effect... 

    Investigation of the Effects of Corrosive Environments on Mechanical and Microstructural Properties of Polymer and Portland Cement Concrete

    , M.Sc. Thesis Sharif University of Technology Ghassemi, Pedram (Author) ; Toufigh, Vahab (Supervisor)
    Abstract
    Polymer concrete is well-known for the quick repair of concrete structures and pavement. Many concrete structures such as bridges, offshore, and pavements are under cyclic loads when they are exposed to different environmental conditions during their lifespan. However, there are relatively few studies on the durability of Polymer concrete. The durability and fatigue performance of these structures are significant issues that should be considered. This study aims to investigate the long-term environmental effects on the mechanical properties of Polymer concrete. Therefore, polymer and ordinary cement concrete specimens were prepared and exposed to four chemical solutions with pH values of... 

    Evaluation of Deformation and Formability Behaviors of the Ferritic-Pearlitic Steel Sheets by Employing the Experimental Approaches and Micromechanical Modeling

    , Ph.D. Dissertation Sharif University of Technology Isavand, Samaneh (Author) ; Assempour, Ahmad (Supervisor)
    Abstract
    A broad range of plain carbon steels have ferrite-pearlite microstructures, which are used in many industrial applications due to the good strength and formability provided by the typical combination of ferrite grains and pearlite colonies. The mechanical behavior of ferrite-pearlite steels inherently originates from the configurations of ferrite grains and pearlite colonies, which comprised alternating lamellae of cementite with randomly distributed orientations in a ferrite matrix. In this thesis, three different experimental-numerical approaches were employed to investigate the deformation behavior, damage mechanisms, and formability of the ferrite-pearlite steels. At the first step, two... 

    Capturing Co2 of the Atmosphere by Molten Carbonates and Transforming to Carbon Nanofiber

    , M.Sc. Thesis Sharif University of Technology Zarei, Mohammad Mahdi (Author) ; Moosavi, Ali (Supervisor) ; Nouri Borujerdi, Ali (Supervisor)
    Abstract
    Capturing the atmospheric CO2 and turning it into value added products is a topic that has been extensively studied in recent years. One of the methods through which CO2 is valorized is via converting it into carbon nanofiber, CNFs. CNFs can be an important material in future human activities due to its valuable properties such as wide range of electrical conductivity, their superior flexibility and strength, But it is currently obstructed in use due to the high cost of manufacturing and the complexity of the synthesis. Furthermore, in today's world, human life is heavily influenced by greenhouse gases, and avoiding emitting gases like CO2, is almost infeasible. This thesis provides an... 

    Synthesis and Investigation of Antistatic Coating Properties Based on Tin Oxide by Sol-Gel Method

    , Ph.D. Dissertation Sharif University of Technology Zakerizadeh, Ali Mohammad (Author) ; Dolati, Abolghasem (Supervisor) ; Abdollah Afshar (Supervisor)
    Abstract
    In order to prevent electrostatic attraction on non-conductive surfaces, the most practical solution is to put antistatic coatings to reduce surface resistance. Nano tin oxide coatings are designed to produce surfaces with antistatic properties in the resistance range of 108-1012 Ω/cm. In this project, using a simple method, low temperature, without heat treatment and without the use of additive (dopant), tin oxide films with antistatic property were placed on the glass. Further, in order to obtain a coating with a suitable morphology and structure to increase the surface conductivity, the synthesis of tin oxide using the sol-gel method at ambient temperature was used. And to place the... 

    Microstructure Modification and Electrical Conductivity Development in PA6/PS Blend using PANI Coated CNT

    , M.Sc. Thesis Sharif University of Technology Soleimani, Elahe (Author) ; Bagheri, Reza (Supervisor)
    Abstract
    In this research, a nanocomposite blend of polyamide 6/polystyrene containing polyaniline-coated carbon nanotubes was fabricated via melt blending method, aiming to achieve electrical conductivity in the range of static dissipation. The effect of weight percentage of nanofillers and surface modification of carbon nanotubes with polyaniline on the electrical properties and microstructure of the nanocomposite was investigated. To promote compatibility between the immiscible polyamide 6 and polystyrene polymers, PS-g-MA compatibilizer was utilized, and its effect on the morphology of the nanocomposite blend was examined. Additionally, the influence of weight percentage of nanofillers and the... 

    Investigation and Synthesis of Zn-Ni-Mn Three Cationic Electrophosphate Coating

    , M.Sc. Thesis Sharif University of Technology Alimi, Zahra (Author) ; Ghorbani, Mohamad (Supervisor)
    Abstract
    The purpose of this study was to create a three-cationic electro phosphate coating of zinc-nickel-manganese by cathodic method and to investigate the effect of operating variables on the properties of zinc-nickel-manganese tri-cationic electro phosphate coating. Hence, the effects of variables such as coating acidity, coating thickness, coating temperature, coating time and concentration of manganese were studied in the bath on the properties such as coating morphology, corrosion resistance, coating thickness. Coating morphology was characterized by scanning electron microscopy and corrosion resistance by polarization test. The pH values of 1.4, 1.8, 2 and 2.2 were selected, and the results... 

    Study of Microstructural Changes Associated with Internal Resistance of a Li-ion Battery

    , M.Sc. Thesis Sharif University of Technology Tabean, Saba (Author) ; Asgari, Sirous (Supervisor)
    Abstract
    As one of the main features of Li-Ion batteries, internal resistance severely affects performance and characteristics of these batteries e.g. output power and working voltage. In this study, we tried to understand role of internal resistance on microstructure development and provide a correlative relation between microstructural features and performance of lithium-ion batteries. To catch this target, four types of Li-Ion battery chose, varying cathode type. These batteries were exposed to both normal and severe cycling conditions. Regarding to the key role of current rate on the performance of Li-ion batteries, an extensive research on different types of batteries at various current rates... 

    Study of CdS thin Film Deposition on Single Layer Grapheme using Close Space Sublimation and SILAR Methods

    , M.Sc. Thesis Sharif University of Technology Bagheripour, Amir Hossein (Author) ; Asgari, Sirous (Supervisor)
    Abstract
    Cadmium sulfide (CdS) thin films were successfully fabricated in argon atmosphere on glass slides and Single Layer Graphene(SLG)/Cu foil stack by close space sublimation technique in three different deposition temperatures. Successive Ionic Layer Adsorption and Reaction (SILAR) technique is used as a complementary technique for better and denser layers. Analysis techniques such as Grazing Incident X-ray Diffraction (GIXRD) and Scanning Electron Microscope images were used for structural study of the deposited layers. Polycrystallinity and hexagonal wurtzite structure of the thin films is confirmed. For band gap calculations and for determination of optical behavior of the layers in different... 

    The Effect of Heat Treatment on Microsructure, Hot Tensile Properties and Creep Bihavior of Nickel-based Superalloy CM88Y

    , M.Sc. Thesis Sharif University of Technology Gorji, Morteza (Author) ; Asgari, Sirous (Supervisor)
    Abstract
    The Ni-base superalloy CM88Y has good hot corrosion resistance, high stability and strength at elevated temperature; accordingly, the alloy is used in manufacturing of gas turbine hot components. In most applications, heat treatment is required in order to achieve the desired mechanical properties and corrosion resistance of the working conditions; often three stages of heat treatment is designed for precipitation hardening nickel-base superalloy. In general, the effective parameters of heat treatment cycles includes temperature, time, heating rate and the cooling rate. In this study, the effect of cooling rate from partial solution temperature (second stage of heat treatment) on the... 

    Formation and Investigation of Zinc-Nickel Two Cathionic Electrophospahte Coating Properties on Galvanized Steel

    , M.Sc. Thesis Sharif University of Technology Barati Darband, Ghasem (Author) ; Afshar, Abdollah (Supervisor)
    Abstract
    By using electrophoaphating treatment in the metal coating process, the operating temperature of chemical phosphating bath is decrease and also difficulties with the use of high temperature bath is eliminated. The aim of this study is investigate the effect of operating parameter on coating properties and also investigation the deposition mechanism of Zn-Ni electrophosphate coating. Coating properties such as morphology, corrosion resistance and porosity of the coating characterized using SEM, polarization test and electrochemical method respectively. The values used for pH effect was 1.6,1.8,2 and 2.2 results indicated that by increasing the pH value from 1.6 to 1.8 the icorr decrease from... 

    Improvement of Mechanical Properties of a Mg-Zn alloy using the Micro Alloying Elements

    , M.Sc. Thesis Sharif University of Technology Cheraghi Heyvedi, Hamid (Author) ; Karimi Taheri, Ali (Supervisor)
    Abstract
    The development of new wrought magnesium alloys for automotive industry has increased in recent years due to their high potential as structuralmaterials for low density and high strength/weight ratio demands. However, the poor mechanical properties of the magnesium alloys have led tosearch a new kind of magnesium alloys for better strength and ductility.In this research,a new type of magnesium alloy based on Mg-Zn-Si-Ca system has been developed using the permanent gravity casting process. For comparison, an alloy without Siby the same method was also produced. The effects of trace Si addition on the microstructure and mechanical properties in magnesium alloy with composition of... 

    The Effects of Alumina Mole Fraction on Morphology and Mechanical Properties of Ce-TZP/Al2O3 Nanocomposite Produced via Aqueous Combustion Synthesis

    , M.Sc. Thesis Sharif University of Technology Vahdat, Armin (Author) ; Yoozbashizadeh, Hossein (Supervisor)
    Abstract
    In the present study, nanocomposite of Ce-TZP/Al2O3 was synthesized via aqueous combustion synthesis. In order to investigate the effects of alumina on the morphology and the mechanical properties of this nanocomposite, four sample with 20, 40, 60 and 80 mole percent of alumina were prepared. At first, the synthesized powders were characterized with scanning electron microscope and X-ray diffraction technique. Then, in order to determine the effects of alumina mole percent on the mechanical properties of the nanocomposite, the powders were uniaxailly compacted with the press of 250 MPa followed by sintering at the temperature of 1400 °C for 4 hours. The density of the compacted powders was... 

    Solution Combustion Synthesis of Spinel-type (Cu,Co) 3O4 Nanopowder

    , M.Sc. Thesis Sharif University of Technology Ghorbanzadeh, Milad (Author) ; Yoozbashizadeh, Hossein (Supervisor)
    Abstract
    In this study, nano-powders of copper-cobalt spinel (CuCo2O4) were fabricated by solution combustion synthesis (SCS) of Cu and Co nitrates with urea, glycine,acid citric and alanine. The method involved exothermic decomposition of viscous liquid nitrates and the fuel. Products which were synthesized by using this fuels contained less impurity constituents. Duo to low purity, other factors which have influence on synthesis process investigated and observed that pH have key role on process. X-ray diffraction (XRD) patterns gave crystal structure and the existing phases. Particle size distribution and morphology changes were studied by dynamic light scattering (DLS) and field emission scanning... 

    The Effect of Different Parameters on the Production of High Alumina Cetzp Al2o3 Nano Composite Produced by Aqueous Combustion Synthesis

    , M.Sc. Thesis Sharif University of Technology Tashi Shamsabadi, Safar (Author) ; Yoozbashizadeh, Hossein (Supervisor) ; Askari, Masoud (Co-Advisor)
    Abstract
    Combustion synthesis is the best and most effective method for producing ceramic nano-composites which is also a simple and economic way of producing very fine powders with high purity. In this method, a series of combustion reactions named aqueous combustion analysis are used for producing single-phase and nano-composite products ,in which the heat produced in reactions are used for completing the phase . several chemical substances such as glycine ,urea ,ammonium acetate and others are used as combustion agents. In order to obtain optimized nano fuel, we produced alumina powder with multiple combustion percentages and composition of 25%moli ammonium acetate (AA) with 75%moli urea was... 

    Pressing and Sintering of Ce-Tzp-Al¬2o3 Nanocomposite with a High Percent of Alumina And Investigation of Sinter Condition on Morphology

    , M.Sc. Thesis Sharif University of Technology Ameri Shahrabi, Hadi (Author) ; Yoozbashizadeh, Hossein (Supervisor)
    Abstract
    In this project alumina-zirconia-ceria nanocomposite with 80% mol alumina (0.2Ce0.1Zr0.9O2-0.8Al2O3) was produced by solution combustion synthesis method. In the mentioned method, optimal fuel with composition of 75% urea, 25% ammonium acetate, and stoichiometric amount of glycine (0.75U-0.25AA-1G) was used. Moreover, ammonium nitrate as aid combustion was added to optimal fuel. In order to calcinations, nanopowder obtained from combustion synthesis was heated to 500°C for 1 hour and kept at this temperature for 2 hours. To complete heat treatment, the nanopowder was heated to 1150°C for 2 hours and 10 min and kept at this temperature for 2 hours. Then the specimens were pressed at pressure...