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    Facile electrochemical detection of morpholine in boiler water with carbon nanostructures: a comparative study of graphene and carbon nanotubes

    , Article Bulletin of Materials Science ; Volume 45, Issue 2 , 2022 ; 02504707 (ISSN) de Oliveira, S. M ; dos Santos Castro Assis, K. L ; Paiva, V. M ; Hashempour, M ; Bestetti, M ; de Araújo, J. R ; D’Elia, E ; Sharif University of Technology
    Springer  2022
    Abstract
    Two electrochemical sensors based on modified glassy carbon electrodes with carbon nanostructures as graphene (GCE–EG) and carbon nanotubes (GCE–CNT) were evaluated for morpholine analysis. The carbon nanostructures were obtained and characterized using X-ray photoelectron spectroscopy, Raman spectroscopy, X-ray diffraction, transmission electron microscopy, high-resolution transmission electron microscopy and cyclic voltammetry. All spectroscopic and microscopic techniques confirmed the procurement of graphene and CNT. The electrochemical studies proved the efficient behaviour of both electrodes GCE–EG and GCE–CNT in sensing and detection of morpholine via differential pulse voltammetry....