Sharif Digital Repository

A low-carbon steel sheet containing 0.05 C, 0.203 Mn, and 0.0229 Si (all in wt%) was rapidly annealed in a temperature range of 300 °C to 600 °C after severe plastic deformation by using constrained groove pressing (CGP) technique. Microstructure evolution was investigated by scanning electron and optical microscopes. Mechanical properties were evaluated by hardness measurements and shear punch test. The results showed a thermal stability up to 400 °C where recrystallization did not occur in the specimens even after 7200 s. This thermal stability is in agreement with previously reported results of conventional annealing of the same steel after CGP. However, annealing at 500 °C and 600 °C led... 

The influence of solution treatment on precipitation behavior of AEREX™350 was investigated using hardness testing, TEM and SEM. Samples were solution treated at 1050°C and 1075°C for 1 hr and then aged at 700°C, 750°C and 800°C for 1,2,4,8 and 25 hrs. It was found that different solution treatment may be used for different applications of AEREX™350  

Utilizing the differential scanning calorimetry (DSC) and Vickers hardness tests, the relationship between the stored energy and indentation hardness of copper after compression test is achieved experimentally. Three dislocation models are utilized to develop the relationships between the stored energy and hardness for justifying the experimental relationship. The relationships show that the stored energy is increased by increasing the hardness, non-linearly. By comparing the models' results with the experimental data, the validity of each model at different ranges of hardness is determined. © 2008 Springer Science+Business Media, LLC  

Some mechanical and metallurgical properties of hollow and solid long forged products are compared. The metallurgical properties include such micro- and macro-structural characteristics as the grain size and grain flow patterns. Mechanical evaluation was performed by means of hardness testing. Some theoretical analyses were also carried out. The results indicate that the hollow or mandrel forged products possess better properties. Both the mechanical and metallurgical properties are more uniform and homogeneous through the thickness direction in such products. By contrast, in the solid forged parts, there is a gradient in the micro- and macro-structural properties from the surface to the... 

A gas turbine which output 18MW power exploded after 3h of ordinary operation and after 4,785 starts. The turbine's rotor had undergone repair after 77,000 operating hours. A piece was cut from the failed marriage bolt and tested using atomic absorption spectrometry in order to know the grade of the alloy. It was found that the marriage bolt is made from ASTM A193 B16 steel which is suitable. Hardness and microhardness measurement was also determined and showed that it was within the range of the specified hardness for ASTM A193 B16 steel. The marriage bolt's mechanical properties also meet technical specifications and showed that it contained anti-corrosion properties. Visual examination... 

To improve the strength and toughness of AISI 4340 steel, different microstructures, containing full bainite, bainite-ferrite, martensite-ferrite and full martensite were produced by different heat treatment cycles. Tensile, impact and hardness tests were carried out at room temperature. The ductile-brittle transition temperature was determined from impact data at different temperatures. The results showed that steel with bainite - 0.34 ferrite microstructure has the highest elongation and charpy impact energy, while its tensile strength and yield stress decreased in comparison to other microstructures. This increment was noticeable when bainite - 0.34 ferrite steel was tempered. The... 

The recrystallization behavior of a commercial nickel-cobalt base superalloy, AEREX 350, is investigated by means of hardness test, X-ray diffraction, and microscopy. It is found that the alloy resists recrystallization up to a high temperature of 1025 °C. Recrystallized grains are readily formed at grain boundaries below this temperature; however, the growth of these new grains is inhibited by Widmanstätten η particles having coherent facets with the nickel matrix (γ). The passage of the recrystallization front results in coherency loss and consequently dissolution of the η platelets. Recrystallization proceeds with a discontinuous precipitation of the η phase behind the moving boundary  

In this research, the welding characteristics of a new UHSLA steel, 35NiCrMoV123, have been studied in two general conditions (annealed and quench-tempered). Carbon equivalent value of 35NiCrMoV123 steel is near 0.9 which classifies it as a "very difficult to weld" steel. The effects of welding heat treatment cycle (preheat, interpass, and postheat) on metallurgical and mechanical properties of weldments have been investigated by tensile, impact toughness, and hardness tests, as well as optical microscopy observations. It has been observed that by employing high-temperature stress relief (600 °C), welding could be performed in annealed condition successfully. Also, the results indicate that... 

In this paper dynamic strain ageing behavior in an Al-Mg-Si alloy related to equal channel angular pressing (ECAP) was investigated. In order to examine the combined plastic deformation and ageing effects on microstructure evolutions and strengthening characteristics, the Al6061 alloy were subjected to φ=90° ECAP die for up to 4 passes via route Bc at high temperatures. For investigating the effects of ageing temperature and strain rate in ECAP, Vickers hardness tests were performed. The combination of the ECAP process with dynamic ageing at higher temperatures resulted in a significant increase in hardness. The microstructural evolution of the samples was studied using electron... 

A high quality joint of zinc based pressure die cast alloys can be hardly achieved by conventional fusion welding. In this study, a novel technique to achieve the globular weld structure using stirring the localized semisolid zone during butt joining of Zamak-3 pressure die cast alloy is proposed and effect of welding parameters on mechanical and microstructural properties are investigated. A gas heating system was designed to heat up the nitrogen gas to desired temperature accurately to create a localized semisolid pool. At this stage a fine stirrer was introduced into the weld seam in order to mix the two sides into a single uniform joint. By presented process, globular microstructure of... 

The effects of warm rolling parameters on the final microstructure and mechanical properties of a low-carbon steel were investigated. In doing so, the steel strips were pre-heated at various temperatures and rolled at different reductions and rolling speeds. Then, microstructural studies were performed and, also, the mechanical properties of the rolled samples were measured by tensile and hardness testing. An optimum rolling program was determined with the aids of experimental results and a mathematical model based on the finite element method (FEM) developed for the warm rolling conditions. The results show that, at high temperatures and low rolling speeds, the roll forces are reduced;... 

Alg -(1, 3, 5, 7, 10 vol%) SiC nanocomposites were produced by mechanical alloying (MA) and double pressing/sintering route. The characteristics of the milled powders and the consolidate specimens were examined using high resolution scanning electron microscopy and X-ray diffraction method. Compression and hardness tests were used to study the effect of SiC volume fraction on the strength of Alg -SiC nanocomposites. It was shown that with increasing the SiC volume fraction, finer particles with narrower size distribution and smaller crystallite size are obtained after MA. During sintering close to the melting point of aluminum, the presence of nanometer-scaled SiC particles was found to... 

The present paper deals with different effects of homogenization time and cooling environment on Ni-42.5wt%Ti-7.5wt%Cu alloy. The alloy was prepared by vacuum arc melting. Afterwards, three homogenization times (half, one and two hour) and three cooling environments (water, air and furnace) at 1373 K were selected. Optical and Scanning Electron Microscopic methods, EDX, DSC and hardness tests have been used to evaluate the microstructure, transformation temperatures and hardness. Results indicate that specimens that were cooled in air are super-saturated. Also, the microstructure from furnace cooling has many disparities with the other cooling environments' microstructure and two types of... 

4340 steel bars were austenitized at 850 °C for 1 h followed by heating at 700 °C for 90 min and quenching into a salt bath at the temperature range of 300-450 °C for 1 h to obtain dual structures with 34 vol.% fraction ferrite and various bainite morphologies. SEM studies showed that by increasing the austempering temperature, bainite morphology varies from lower to upper bainite. Tensile, impact and hardness tests revealed that increasing the austempering temperature from 300 to 400 °C leads to a reduction in yield and ultimate tensile strength, hardness, uniform and total elongation and impact energy. But in dual phase steel produced by austempering at 450 °C, yield and tensile strength... 

In this study a severe plastic deformation method called constrained groove pressing (CGP) is used for imposing a high magnitude of strain into the low carbon steel sheets. Microstructural changes during process are examined by X-ray diffraction and optical observations. The grain size evolution during severe plastic deformation is studied using Williamson-Hall analysis on XRD pattern of the deformed samples. In effective strain of 4.64, ferrite grains with a submicron size of 200-300nm are achieved. The results show that constrained groove pressing can effectively refine the coarse-grained structure to an ultra fine grain range. Mechanical properties changes due to microstructure evolution... 

Carbide morphologies of white cast iron containing 22% Cr and 10-12% tungsten with different carbon contents (2.34-3.20. wt.%) were investigated. Results indicated that for the as-cast alloys with no heat treatments, the addition of carbon changes the morphology of carbides during air-cooling in the presence of tungsten. Light microscopy analysis revealed that for an alloy with 2.3. wt% carbon, chromium carbides possess coarse gray appearance (GA). Increasing the carbon content reduced the coarse GA zones volume fraction while a finer GA zones emerged. The coexistence of coarse and fine GA phases came to an end at 2.8. wt% carbon, at which only fine GA zones spread throughout the chromium... 

Effects of cold rolling on the microstructure and mechanical properties of Fe-Ni-Mn-Mo-Ti-Cr maraging steels were studied. To investigate the microstructure and mechanical properties, optical microscopy, scanning electron microscopy, X-ray diffraction, tensile test, and hardness test were used. The results show that the solution-annealing treatment in the cold-rolled steel redounds to the formation of submicrocrystalline Fe2 (Mo, Ti) Laves phase particles, which are stable at high temperatures. These secondary Laves phase particles prevent from recrystallization at high temperatures and correspond to semi-brittle fracture in the subsequent aging treatment  

In this study, hot extrusion of AA6061-5% SiCp composite was studied to determine the composite thermo-mechanical behaviour during deformation and the mechanical properties of extruded composite. Hot compression tests were first carried out to obtain the flow stress behaviour of the composite at different temperatures and strain rates. Then a mathematical model was used to estimate the required energy as well as to predict temperature and strain distributions during the process. Finally, hot extrusion experiments were performed in order to verify the predictions and, also, tensile and hardness testing were conducted to evaluate mechanical properties of extruded material. Comparison between...