Sharif Digital Repository

Al-15wt.% Mg2Si composites were prepared by in situ casting and characterized in wear tests. Previous to the extrusion of specimens at 470°C - varying extrusion ratio (7.4, 14.1 and 25), the as-cast composites were homogenized at 500°C for 5h, followed by slow furnace cooling. The microstructure, hardness and sliding wear behavior were characterized for both, the as-cast and hot extruded composites. Results show that increasing the extrusion ratio causes a significant improvement in hardness and wear resistance. This is ascribed to the observed decrease in average size and better distribution of Mg2Si particles, in tandem with a remarkable decrease in porosity percentages, which goes from... 

In this study, we attempt to characterize the microstructural evolution during friction stir butt welding of Al-Cu-laminated composites and its effect on the fracture behavior of the joint. Emphasis is on the material flow and particle distribution in the stir zone. For this purpose, optical microscopy and scanning electron microscopy (SEM) images, energy-dispersive spectroscopy EDS and XRD analyses, hardness measurements, and tensile tests are carried out on the joints. It is shown that intermetallic compounds exist in lamellas of banding structure formed in the advancing side of the welds. In samples welded from the Cu side, the banding structure in the advancing side and the hook... 

Microstructures and hardness of aluminum alloy ductile iron were investigated by SEM, XRD, EPMA and hardness measurement techniques. The results show, increasing the Al-alloying element leads to decrease of free ferrite and carbide, as well as increase in the pearlite volume fraction. It is also has been found that in the higher values of Al, about 85% of the matrix would be pearlite. It is indicated that an increase in the aluminum content also leads to a decrease in the spacing between pearlite layers. XRD results show, in the presence of Al, intermetallic compounds such as Al6Fe, AlFe3C0.5, Fe3Al and FeAl were produced. Furthermore the hardness measurements illustrate that by increasing... 

In the present work, ultrafine-grained Al-5vol.% Al2O3 nanocomposite was synthesized through mechanical milling followed by direct powder extrusion method. The characteristics of the processed nanocomposite were examined by electron microscopy (SEM and TEM), Xray diffraction (XRD), tensile test and Vickers hardness measurement. It was shown that the addition of the reinforcement nanoparticles accelerates the milling process of the aluminum matrix and enhances the grain refinement of the aluminum matrix. An improved mechanical strength as compared with Al-Al2O3 microcompoiste was obtained. A dimple-type fracture mode was observed, which is a clear evidence of micro-deformation. In addition,... 

Mechanical properties, microstructural events, residual stresses, and aging behavior of friction stir-welded AA6061-T6 were investigated in this work. Microstructural and mechanical characterizations of the friction stir-welded joints in as-welded and post-welded conditions were made by means of optical metallography, transmission electron microscopy, X-ray diffraction for determination of residual stresses, tensile testing, and hardness measurements. It was found that weld strength and hardness variations after welding are mainly dependent on the imposed heat input per unit length. Besides, the kinetics of natural aging in the welded samples was found to be noticeable within the first 14... 

Gas tungsten arc welding of CK45 and AISI304 stainless steel was performed through preparation of different types of samples using ER308L and ERNi-1 wires. Welded samples were studied by different techniques including optical metallography, scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), X-ray diffraction, hardness measurements and impact test. It was observed that in the buttered specimen, the structure of the weld metal was completely austenitic while the microstructure of unbuttered sample was duplex ferritic-austenitic. M23C6-type carbides were observed within the weld metal of both as-weld specimen types. Effects of different post-weld heat... 

In this study, the kinetics of aging in AA6061 and AA6061 with 5% volume fraction SiCp were studied and compared. The composite was first produced and homogenized using stir casting technique followed by hot extrusion with the ratio of 18:1. Then, both AA6061 and the composite were aged at three different temperatures including room temperature, 170 °C and 240 °C, while mechanical properties during aging were evaluated employing hardness measurements and tensile testing. Moreover, in order to assess the effect of plastic deformation on the kinetics of aging, a series of samples were first deformed by equal-channel angular pressing immediately after solution treatment and then aged in the... 

Aluminum metal-matrix nanocomposites (AMMNCs) fabricated by conventional stir-casting process usually show high porosity and poor distribution of nanoparticles within the matrix. In the current study, for the improvement of nanoparticles distribution in the aluminum matrix and enhancement of the mechanical properties, a mixture of Al/nano-Al2O3 powders were injected by pure argon gas into the molten 7075 aluminum alloy and this mixture was extruded at high temperature. Mechanical behavior of the final product was investigated by tensile and compression tests, hardness measurements, Scanning Electron Microscopy (SEM), High Resolution Transmission Electron Microscopy (HRTEM) and Optical... 

In this study, the effects of pulse current mode on corrosion resistance and mechanical properties of anodized coatings were explored. Thickness and hardness measurements, polarization and electrochemical impedance spectroscopy were employed to take mechanical and corrosion behaviors of the anodized coatings into consideration. Also, field-emission scanning electron microscopy (FE-SEM) was utilized to characterize the surface morphology of the coatings. It was shown that in short anodizing times, coating thickness is controlled by the heat concentrated on coating. Although at prolonged anodizing times, the coating thickness is affected by average current density. Hardness measurements showed... 

In this study, the effect of surface modified nano-zirconia (nano-ZrO2) on the corrosion protection of epoxy coating on mild steel was investigated. An organosilane (trimethoxy methyl silane) was used as a surface modifier to improve the dispersability of the inorganic nanoparticles in the organic coating matrix. Fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TGA) were used to characterize the sol-gel surface modified nanoparticles. The dispersability of the modified and unmodified nano-zirconia in an epoxy coating was examined by field emission-scanning electron microscopy (FE-SEM). Electrochemical impedance spectroscopy (EIS) and salt spray were employed to... 

In this study, the effects of pulse current parameters on corrosion resistance and mechanical properties of anodized coatings were evaluated. Hardness measurements, polarization and electrochemical impedance spectroscopy tests were employed to investigate the mechanical properties and corrosion behavior of these coatings. Also, field emission scanning electron microscopy (FE-SEM) was used to analyze the surface morphology and microstructure of the coatings. It was found that the properties of anodized coatings were dependent on various parameters, among which, time, temperature and pulse current parameters (current density limit, frequency and duty cycle) were optimized. Analysis of Variance... 

In this study, the effect of surface modified silver nanoparticles on the corrosion protection of an epoxy coating on mild steel was studied. An organosilane (3-methoxy silyl propyl metacrylate) was used as a surface modifier to increase the dispersability of the inorganic nanoparticles in the organic epoxy coating matrix. Fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TGA) were used to characterize the surface modified nanoparticles. Differential scanning colorimetry (DSC) was employed to study the effects of modified and unmodified nano-silver on the curing heat and glass transition temperature of the epoxy coatings. Salt spray and electrochemical impedance... 

Aluminum metal-matrix nanocomposites (AMMNCs) fabricated by conventional stir-casting process usually show high porosity and poor distribution of nanoparticles within the matrix. In the current study, for the improvement of nanoparticles distribution in the aluminum matrix and enhancement of the mechanical properties, a mixture of Al/nano-Al2O3 powders were injected by pure argon gas into the molten 7075 aluminum alloy and this mixture was extruded at high temperature. Mechanical behavior of the final product was investigated by tensile and compression tests, hardness measurements, Scanning Electron Microscopy (SEM), High Resolution Transmission Electron Microscopy (HRTEM) and Optical... 

In this work, static strain aging behavior of an alloy steel containing high amounts of silicon and manganese was examined while the influences of initial microstructure and pre-strain on the aging kinetics were evaluated as well. The rate of strain aging in a low carbon steel was also determined and compared with that occurred in the alloy steel. The rates of static strain aging in the steels were defined at room temperature and at 95 °C by means of double-hit tensile testing and hardness measurements. In addition, three-stage aging experiments at 80 °C were carried out to estimate aging behavior under multi-pass deformation processing. The results showed that in-solution manganese and... 

A series of samples with different compositions and parameters were welded together. The alloys were based on Ni-8Al-8Cr-l.5Mo-0.01B %wt composition with Zr additions of 1 and 3 %wt. Crack-free full-penetration welds of castable nickel aluminide alloy were performed using autogenous GTAW technique. It was found that Ni-Ni5Zr eutectic was associated with solidification cracks. Alloys were fully dendritic and also, weld metal consisted of columnar and axial dendrites beside the fusion line and in the middle, respectively. Optical and scanning electron microscopy (SEM) techniques were employed to characterize the composition as well as the weld structure. X-Ray diffraction was utilized to... 

The effects of initial heat treatments, i.e. solution treating and over ageing, on deformation behavior of an age hardenable Al-Cu-Mg alloy, including mechanical properties and texture evolution, during multi-directional forging (MDF) are investigated. Hardness measurements, electron back scatter diffraction (EBSD) maps, and differential scanning calorimetry (DSC) are carried out. Mechanical behaviors of the alloy in terms of compressive stress and hardness test after MDF are investigated. In both solution treated and over-aged alloys, the compressive stress during MDF shows an increase up to the second pass, and by further straining the flow stress is decreased. However, shear and... 

Different microstructures were produced by heat treatment of 4340 steel. These microstructures are bainite, martensite, ferrite-martensite and ferrite-bainite. Mechanical tests were carried out at room temperature. The results showed that steel with bainite-ferrite microstructure has better ductility and charpy impact energy than steels with martensite-ferrite and full bainite microstructures. But yield and tensile strengths of this steel are less than the yield and tensile strengths of the other two steels. Hardness measurements showed that their hardness is the same. Fracture surface observations of tensile specimens showed increase in toughness of bainite-ferrite in comparison to... 

An Al2O3/Si3N4 nanocomposite coating was successfully fabricated on commercial aluminum alloy. Hardness measurements, polarization and electrochemical impedance spectroscopy (EIS) were employed to study the mechanical and corrosion behaviors of the coatings. Field-Emission Scanning Electron Microscopy (FE-SEM) equipped with Energy Dispersive Spectroscopy (EDS) and X-ray diffraction (XRD) were utilized to characterize the surface morphology and phase composition of the coatings. Also, coatings abrasive wear properties were evaluated with a modified ASTM G105 standard. FE-SEM image, EDS and XRD analysis revealed the presence of Si3N4 in the coating. Furthermore, the results showed hardness of... 

In this work, nanocrystalline Al6063 composite powder reinforced with nanometric oxide ceramic particles was synthesized via an in situ solid-gas reaction during high-energy mechanical alloying under a mixture of argon-oxygen atmosphere. The effect of oxygen volume fraction on the morphological evolution and microstructural changes during mechanical alloying was studied by various analytical techniques including optical and electron microscopy, X-ray diffraction, laser particle size analysis, apparent density measurement, and microhardness test. The reactive mechanical alloying resulted in the formation of amorphous Al- and Al-Mg-Si-Fe oxides with a size range of 40-100. nm and volume...