Sharif Digital Repository

A novel method is proposed in order to find the kinetics of dynamic recovery in the form of Avrami relation using hot flow curves. The relation is derived on the basis of variation of dislocation density with strain. The model is applied on an Al-Mg alloy  

Kinetics of crystallization in an amorphous (Fe0.5Co 0.5)77Si11B9Cu0.6Nb 2.4 (at.%) alloy was investigated using differential scanning calorimetry (DSC). Transformed fraction as a function of temperature was obtained by accurate DSC measurement and the experimental data analyzed with Vyazovkin model-free kinetic method. Reconstructed form of the experimental kinetics model, g(α), clearly showed the crystallization mechanism do not belongs to a single model but almost follows the Avrami-Erofe'ev. Magnetic coercivity and hysteresis loss values of the annealed samples at 823 K were 7.5 A m-1 and 1.2 J m-3, compared to 17.1 A m-1 and 37.1 J m-3 for as spun samples. Magnetic measurements show the... 

The effects of melt quality and the placement of a filter in the filling system on Weibull distributions of tensile strength and elongation of Al-7%Si-Mg alloy castings were investigated. Three different combinations of melt quality and filtering were used: (a) unstirred, with filter in the filling system, (b) stirred to produce and entrain surface oxide films with no filter in the filling system to emulate poor initial melt preparation and melt handling, and (c) stirred and with a filter placed in the filling system. The results showed that the highest elongation and tensile strength values were obtained from the unstirred, filtered condition and lowest values were from stirred and... 

This paper addresses solidification and solid state precipitation phenomena during transient liquid phase (TLP) bonding of wrought IN718 nickel base superalloy using Ni-4.5Si-3.2B (wt.%) ternary filler alloy. The solidification sequence of the residual liquid in the joint centerline was found to be (1) formation of proeutectic γ, followed by (2) γ/Ni3B eutectic reaction, followed by (3) ternary eutectic of γ/Ni 3B/Ni6Si2B. Extensive fine Ni3Si formed within the eutectic-γ via solid state precipitation during cooling. Extensive Cr-Mo-Nb rich boride precipitates were formed in the substrate region due to boron diffusion into the base metal during bonding process. The implications of the phase... 

The present study investigates the evolution of γ′ precipitate microstructure in a creep damaged IN738LC superalloy during different stages of rejuvenation heat treatment cycles. Dissolution of coarsened γ′ precipitates in the creep damaged alloy occurred during different solution treatments. The precipitates that did not dissolve completely during solution treatment and those formed during subsequent cooling were considered to be as remnant and cooling precipitates respectively. It was found that higher solution treatment temperatures result in lower volume fraction of remnant precipitates and further formation of cooling precipitates. Slower cooling rates after solution treatment gave the... 

In this paper, an introduction of the finite element approach to microstructure based modelling is provided, and the primary and secondary dendrite arm spacings of A356 alloy in the solidification process are simulated. The simulated results of dendrite morphology and the experimental measurements are presented and compared with the investigations of other researchers, which confirmed the accuracy of this model in its ability to predict the dendrite arm spacing. Each of the length scales, including silicon rod diameter and spacing, is discussed in detail. Analytical equations are generated for the length scales and incorporated in the Sharif University Technology academic software for the... 

Multilayer laser cladding process for the material properties of low carbon steel 1015 for workpiece and nickel alloy with 1.5 wt.% and 3 wt.% nano CeO2 as the powder particles is modeled. Finite Element Method (FEM) solutions of transient heat transfer and mass transfer equations in laser cladding process are presented. Geometry of the deposited material as well as temperature and thermal stress fields across the process area are calculated  

The logarithmic or Hencky strain measure is a favored measure of strain due to its remarkable properties in large deformation problems. Compared with other strain measures, e.g.; the commonly used Green-Lagrange measure, logarithmic strain is a more physical measure of strain. In this paper, we present a Hencky-based phenomenological finite strain kinematic hardening, non-associated constitutive model, developed within the framework of irreversible thermodynamics with internal variables. The derivation is based on the multiplicative decomposition of the deformation gradient into elastic and inelastic parts, and on the use of the isotropic property of the Helmholtz strain energy function. We... 

Transient liquid phase (TLP) bonding of Al2024-T6 alloy, using gallium (Ga) interlayer, has been investigated. Bonding process was carried out at 470°C for 6 min, and homogenising temperature and time were 495°C and 2 h respectively. Conventional TLP bonding using Ga interlayer was not an appropriate method for joining of Al2024. In this method, the boundary between two Al2024 specimens was not fully eliminated during bonding because of solidification with planar front. In addition, bonding zone was depleted of copper, and as a result, tensile and shear strength of joint decreased to 200 and 110 MPa respectively. TLP bonding under temperature gradient offered very good results in bonding of... 

The ever increasing number of shape memory alloy applications has motivated the development of appropriate constitutive models taking into account large rotations and moderate or finite strains. Up to now proposed finite-strain constitutive models usually contain an asymmetric tensor in the definition of the limit (yield) function. To this end, in the present work, we propose an improved alternative constitutive model in which all quantities are symmetric. To conserve the volume during inelastic deformation, an exponential mapping is used to arrive at the time-discrete form of the evolution equation. Such a symmetric model simplifies the constitutive relations and as a result of less... 

In this paper we investigate a three-dimensional finite-strain phenomenological constitutive model and propose an efficient solution algorithm by properly defining the variables and by avoiding extensively-used regularization schemes which increase the solution time. We define a nucleation-completion criterion and modify the regularized solution algorithm. Implementation of the proposed integration algorithm within a user-defined subroutine UMAT in the commercial nonlinear finite element software ABAQUS has made possible the solution of boundary value problems. The obtained results show the efficiency of the proposed solution algorithm and confirm the improved efficiency (in terms of... 

In the present research work the binary NiTi alloys with various compositions in the range of 50.3-51 at.% Ni were used. Samples have been annealed at 850 °C for 15 min and then quenched in water. In order to characterize transformation temperatures and enthalpy changes of the forward and the reverse martensitic transformation, Differential Scanning Calorimetric (DSC) experiments were performed. The enthalpy and entropy changes as a function of Ni atomic content have been thermodynamically investigated. Results show that enthalpy and entropy changes of martensitic transformation decrease when Ni atomic content increases. The variation of enthalpy and entropy of martensitic transformation... 

An age-hardening model has been developed to predict the evolution of the hardness of Al-Mg-Si alloys during non-isothermal ageing before peak age. The concurrent precipitation and dissolution have been considered in the structural model. Then the structural model has been combined with strengthening model to predict the precipitation-hardening behavior of the alloy AA6061. The results indicate that the developed model can be used as a predictive tool to model the mechanical properties evolution of Al-Mg-Si alloys during non-isothermal heat treatment. © 2008 Elsevier B.V. All rights reserved  

A high quality joint of zinc based pressure die cast alloys can be hardly achieved by conventional fusion welding. In this study, a novel technique to achieve the globular weld structure using stirring the localized semisolid zone during butt joining of Zamak-3 pressure die cast alloy is proposed and effect of welding parameters on mechanical and microstructural properties are investigated. A gas heating system was designed to heat up the nitrogen gas to desired temperature accurately to create a localized semisolid pool. At this stage a fine stirrer was introduced into the weld seam in order to mix the two sides into a single uniform joint. By presented process, globular microstructure of... 

In this study the influence of precipitates on the mechanical properties and plastic anisotropy of an age hardenable aluminum alloy during uniaxial loading was investigated using crystal plasticity modeling. The kinetics model of Myhr et al. was used to obtain the solute and precipitate features after different cycles of aging treatment. The amounts of solute, precipitate size and volume fraction, and dislocation density varying during deformation, were used to calculate the slip system strength. An explicit term was obtained based on the elastic inclusion model for the directional dependency of internal stress developed by non-shearable rod shape precipitates. Also, a dislocation evolution... 

The corrosion behavior of different grades of commercial aluminum such as AA1040, AA5083, AA6060 and AA7075 in ZnO-containing 4 M NaOH has been determined by using open circuit potential-time measurements (OCP), galvanostatic and potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The results of scanning electron microscopy (SEM) and energy dispersive analysis of X-ray (EDAX) reveal that ZnO produces the inhibition effect by the formation of a zinc-containing deposit layer on the surface of aluminum electrodes. Although the influence of zincating on the performance of aluminum alloys and considering the amount of alloying elements such as zinc, magnesium and... 

Hot compression tests were carried out on a Fe-29Ni-17Co alloy in the temperature range of 900 °C to 1200 °C and at strain rates of 0.001-1 s-1. Dynamic recrystallization was found responsible for flow softening during hot compression. The flow behavior was successfully analyzed by the hyperbolic sine equation and the corresponding material constants A, n and α were determined. The value of apparent activation energy was determined as 423 kJ/mol. The peak and steady state strains showed simple power-law dependence on the Zener-Hollomon parameter. The dynamic recrystallization kinetics was analyzed using Avrami equation and the corresponding exponent was determined to be about 2.7. This... 

The variation of morphology and mechanical properties of Al6061 automotive aluminum alloy due to friction stir welding (FSW) and gas tungsten arc welding (GTAW) was investigated by optical metallography, scanning electron microscopy, microhardness measurement, X-ray diffraction, tensile testing, and fractography. The center-line dendrite emergence and microhardness reduction in the heat-affected zone were observed in the GTAW process. Although similar microhardness reduction with respect to the base metal was observed in the FSW samples, higher HVs were obtained for the FSW rather than the GTAW process at almost all heat-affected locations. Ultimate tensile strengths of the FSW and the GTAW... 

Gas porosities and Fe-rich phases and entrapped double oxide films (hereafter: oxides) are known to be the most detrimental defects in cast Al-Si-Mg alloys. The effects of H (gas porosities) and Fe (Β-Al5FeSi phase) on reproducibility of tensile properties in Al-7Si-0.35Mg alloy have been investigated in this study. Four different casting conditions (Low H-Low Fe, Low H-High Fe, High H-Low Fe and High H-High Fe) were studied. In each case, 30 tensile test samples were prepared by casting in a metallic mold and machining (total of 120 tensile test samples). Results of tensile test were analyzed by Weibull three-parameter analyses. The microstructures of samples were studied by optical... 

In conventional grinding of hard to cut materials such as Ti6Al4V alloys, surface burning, redeposition and adhesion of chips to the grinding wheel and workpeice occur visibly unless it is carried out at low speeds and with high volume of cutting fluid. Ultrasonic assisted grinding is an efficient machining process which improves the machinability of hard-to-cut materials by changing the kinematics of the process. In this research, the effect of imposition of ultrasonic vibration on the grinding of Ti6Al4V alloy is studied. Longitudinal vibration at ultrasonic frequency range (20 kHz) is applied on the workpiece and machining forces and surface roughness are compared between conventional...