Sharif Digital Repository

This paper focuses on characterization of intervertebral disc behavior upon fatigue stress. It consists in in-vitro experiments to measure intervertebral disc deformation with regard to forces applied to produce fatigues test. In this paper, a system modeling based non-invasive method to assess back pain is proposed which may be used for designing of prediction model to predict the failure of intervertebral disc (IVD) experiencing fatigue loading. An artificial compression fracture was simulated in the lower level of vertebra followed by a poly(methyl methacrylate) (PMMA) bone cement injection. Fatigue loading was applied on the specimens and the load was incrementally increased form 650 N... 

This study focuses on a forward looking approach in which deep eutectic solvents (DESs), a new class of designer solvents, were impregnated into micro porous polyvinylidene fluoride (PVDF) membrane for the separation of CO2 from CH4. Three types of DESs were prepared by mixing and heating of hydrogen bond acceptor (choline chloride) with either malic acid, tartaric acid or oxalic acid as hydrogen bond donor. The Fourier transform infrared spectroscopy confirmed the hydrogen bond interactions in the resulting DES. Thermal gravimetric analysis (TGA) was used to evaluate the thermal stability of the prepared membranes. The DES based supported liquid membranes were investigated systematically to... 

Pr and Co co-doped BiFeO3 multiferroics of the following composition BiCoxPrxFe1-2xO3, where (x = 0.00, 0.05, 0.10, 0.15, 0.20 and 0.25) were prepared via sol-gel route. XRD, FTIR, SEM, VSM and VNA were used to evaluate the structural, phase, morphological and electromagnetic properties of Pr and Co co-doped multiferroics. All the undoped and Pr–Co co-doped multiferroics were of single rhombohedral phased whereas at higher concentration the orthorhombic structure was present. FTIR analysis exhibited the presence of orthorhombic phase. SEM images revealed that the grains of Pr and Co doped multiferroics are circular and elliptical in shape. Dielectric and electromagnetic properties were... 

Pr and Co co-doped BiFeO3 multiferroics of the following composition BiCoxPrxFe1-2xO3, where (x = 0.00, 0.05, 0.10, 0.15, 0.20 and 0.25) were prepared via sol-gel route. XRD, FTIR, SEM, VSM and VNA were used to evaluate the structural, phase, morphological and electromagnetic properties of Pr and Co co-doped multiferroics. All the undoped and Pr–Co co-doped multiferroics were of single rhombohedral phased whereas at higher concentration the orthorhombic structure was present. FTIR analysis exhibited the presence of orthorhombic phase. SEM images revealed that the grains of Pr and Co doped multiferroics are circular and elliptical in shape. Dielectric and electromagnetic properties were... 

The X-ray photoemission (XPS) measurements of Cu1-xTlxBa2Ca2 Cu3-yZnyO10-δ (y = 0, 2.65) superconductors have been performed and compared. These studies revealed that the charge state of thallium in the Cu0.5Tl0.5Ba2O4-δ charge reservoir layer in Zn doped samples is Tl1+, while it is a mix of Tl1+ and Tl2+ in Zn free samples. The binding energy of Ba atoms in the Zn doped samples is shifted to higher energy, which when considered along with the presence of Tl1+ suggested that it more efficiently directed the carriers to ZnO2 and CuO2 planes. The evidence of improved inter-plane coupling witnessed in X-ray diffraction is also confirmed by XPS measurements of Ca atoms in the Zn doped samples.... 

X-ray photo-emission spectroscopy (XPS) studies of Cu1-xTlxBa2Ca3Cu4 O12-y superconductor thin films have been carried out for understanding the mechanism of superconductivity and to find out the reasons for the increase of zero resistivity critical temperature Tc(R = 0) with post-annealing in a nitrogen atmosphere. It is observed from these studies that reduction of charge state of thallium is a source of doping of carriers to the CuO2 planes. The reduced charge state of thallium (i.e. Tl1+) promotes lower oxygen concentration in the charge reservoir layer, which possibly results in movement of electrons to the conducting CuO2 planes. The higher density of electrons in the CuO2 planes... 

As of late quantum calculus is broadly utilized in different parts of mathematics. Uniquely, the hypothesis of univalent functions can be newly portrayed by utilizing q-calculus. In this paper, we utilize our recently presented symmetric p,q-number m p,q to characterize new symmetric p,q-derivative D p,q of analytic function f in the open unit disk U. Utilizing D p,q, we introduce new class of analytic star-like functions and examine some fascinating results. © 2021 Khalid Akbar et al  

As of late quantum calculus is broadly utilized in different parts of mathematics. Uniquely, the hypothesis of univalent functions can be newly portrayed by utilizing q-calculus. In this paper, we utilize our recently presented symmetric p,q-number m p,q to characterize new symmetric p,q-derivative D p,q of analytic function f in the open unit disk U. Utilizing D p,q, we introduce new class of analytic star-like functions and examine some fascinating results. © 2021 Khalid Akbar et al  

Ca-doped Ni–Mg–Mn spinel ferrites with compositions of Ni0·5Mg0·3Mn0.2CaxFe2-xO4 (x = 0, 0.1, 0.2, 0.3, 0.4, 0.5) were prepared via sol-gel auto-ignition technique. TGA/DTA, FTIR, XRD, FESEM, and VSM were employed to evaluate the thermal, spectral, structural, morphological, and magnetic features of Ca-doped Ni–Mg–Mn spinel ferrites. TGA/DTA curves show the weight loss in the sample. This weight loss was attributed to the oxidation and decomposition of the sample contents at a temperature of 500 °C. XRD reveals a single-phase structure of the Ni–Mg–Mn nano ferrites. A single-phase orthorhombic structure was confirmed for Ca-doped Ni–Mg–Mn ferrites. Structural parameters such as lattice... 

The high temperature superconductor thin films Cu1-xTl xBa2Ca3Cu4O12-δ (Cu1-xTlx- 1234) are post-annealed in a nitrogen atmosphere. The zero-resistivity critical temperature (Tc(R ≤ 0)) of these thin films is increased from 92.3 to 104K. The grain size is enhanced and their morphology is improved with the post-annealing. The enlargement of grain size is linked to fluctuation-induced conductivity (FIC) in the light of Aslamazov-Larkin (AL) theory. The FIC measurements have shown that the cross-over of three-dimensional (3D) to two-dimensional (2D) behaviour of fluctuations is shifted to higher temperature values with an increase of post-annealing temperature. These results have shown that the... 

Rare earths (REs) play a key role in distorting spinel structure by creating some defects at the lattice sites and make them suitable for magnetodielectric applications. In the present study, the nanoferrites of CuRE0.02Fe1.98O4, where REs = Y3+, Yb3+, Gd3+, were prepared using one step sol–gel method. The prepared samples are copper ferrite (CFO), yttrium doped copper ferrite (Y-CFO), ytterbium doped copper ferrite (Yb-CFO) and gadolinium doped copper ferrite (Gd-CFO), respectively. The single-phase structure of all the REs doped nanoferrites was determined by X-ray diffraction (XRD) analysis. The porosity, agglomerations and grain size of the REs doped copper ferrite were examined using... 

NiZn nanoferrites doped with rare-earth cations having stoichiometric composition such as Ni0.5Zn0.5R0.02Fe1.98O4 (R = Tb, Pr, Ce, Gd, Y) were prepared by sol–gel technique. The same amount of Ni and Zn with constant ratio of different rare-earths ions were doped to investigate the variations in the properties. X-ray diffraction (XRD), Field emission electron microscope (FESEM), and vibrating sample magnetometer (VSM) were used to investigate the structure, morphology, and magnetic properties of rare-earth doped NiZn nanoferrites, respectively. X-ray density, bulk density, and porosity were also calculated. Phase, crystallite size, structure, d-spacing, lattice parameter, micro strain, and... 

NiZn nanoferrites doped with rare-earth cations having stoichiometric composition such as Ni0.5Zn0.5R0.02Fe1.98O4 (R = Tb, Pr, Ce, Gd, Y) were prepared by sol–gel technique. The same amount of Ni and Zn with constant ratio of different rare-earths ions were doped to investigate the variations in the properties. X-ray diffraction (XRD), Field emission electron microscope (FESEM), and vibrating sample magnetometer (VSM) were used to investigate the structure, morphology, and magnetic properties of rare-earth doped NiZn nanoferrites, respectively. X-ray density, bulk density, and porosity were also calculated. Phase, crystallite size, structure, d-spacing, lattice parameter, micro strain, and... 

Currently, materials with outstanding absorption abilities, such as thin size, better absorbing power, and light weight are the need of industry to resolve the electromagnetic issues. However, the research on optimizing the composition of the material, microstructure and the structure of the absorber are also the important factors for enhancing the absorption features. A metamaterial microwave absorber (MMA) based on nano ferrites with desirable absorption peaks is proposed and simulated. Sol-gel auto combustion route is used to prepare the nanosized Sm doped Co ferrite with Co1+xSmxFe2-2xO4 at x = 0.00, 0.03, 0.06, 0.09, respectively. XRD, VSM, FESEM, and VNA were employed to evaluate the... 

Copper (Cu) substituted Co–]Ce nanoferrites with nominal composition of Co 1-x Cu x Ce 0.05 Fe 1.95 O 4 (x = 0.00, 0.25, 0.50, 0.75, 1.00) were prepared by sol-gel route. The sintering of the Cu doped Co–]Ce nanoferrites was done at 700 °C to investigate the desired properties of the Cu doped Co–]Ce nanoferrites. The combination of transition metal (Cu) and rare earth (Ce) were employed to tailor the characteristics of the spinel ferrites. The constant ratio of rare earth and systematic doping of Cu in Co ferrite was incorporated to see the effects of these ions in spinel ferrite. FTIR, FESEM, XRD and VSM were used to study the vibrational bands, phase, morphology, structure and magnetic... 

NMZ ferrites doped with rare earth having spinel composition Ni0.5Mn0.3Zn0.2X0.02Fe1.98O4, whereas X = Y, Pr and Gd were synthesized by sol gel auto-ignition method. XRD, FESEM, VSM and VNA were used to determine the phase, microstructural, magnetic and electromagnetic properties of rare earths doped NMZ ferrite. XRD analysis confirms the single phase of the rare earths doped NMZ ferrite. FESEM images shows Pr doped NMZ ferrite has less agglomerations and more porous structure as compared to NMZ and other rare earths doped NMZ ferrites. Magnetic analysis shows the enhancement in saturation magnetization and remanence with the doping of Y, Pr and Gd in NMZ ferrite. Dielectric properties were... 

NMZ ferrites doped with rare earth having spinel composition Ni0.5Mn0.3Zn0.2X0.02Fe1.98O4, whereas X = Y, Pr and Gd were synthesized by sol gel auto-ignition method. XRD, FESEM, VSM and VNA were used to determine the phase, microstructural, magnetic and electromagnetic properties of rare earths doped NMZ ferrite. XRD analysis confirms the single phase of the rare earths doped NMZ ferrite. FESEM images shows Pr doped NMZ ferrite has less agglomerations and more porous structure as compared to NMZ and other rare earths doped NMZ ferrites. Magnetic analysis shows the enhancement in saturation magnetization and remanence with the doping of Y, Pr and Gd in NMZ ferrite. Dielectric properties were... 

State estimation in power engineering is used as a tool to find the unknown parameter values from the hypothesized model by utilizing the specified information available about the system. Due to random noises that are added from different sources, the exact value of the state vector cannot be found. This study is an effort to describe the simultaneous and individual confidence intervals for the state parameters in view of the heteroscedastic structure of the error terms. The performance of the constructed intervals in terms of coverage probability has been evaluated by using the Monte Carlo simulation study. The results of the study demonstrate that it is an effective method for practical... 

An energy management system (EMS) was proposed for a campus microgrid (μG) with the incorporation of renewable energy resources to reduce the operational expenses and costs. Many uncertainties have created problems for microgrids that limit the generation of photovoltaics, causing an upsurge in the energy market prices, where regulating the voltage or frequency is a challenging task among several microgrid systems, and in the present era, it is an extremely important research area. This type of difficulty may be mitigated in the distribution system by utilizing the optimal demand response (DR) planning strategy and a distributed generator (DG). The goal of this article was to present a... 

In this study, an attempt has been made using different concentrations of rare-earth (RE) elements Yb, Gd in Ni–Zn spinel ferrite to examine the magneto-optical and electrical conductivity analysis of the prepared samples. RE doped Ni–Zn ferrite with composition Ni0.5Zn0.5YbxGdxFe2-xO4 (where, x = 0.00, 0.20, 0.40, 0. 60, 0.80 and 1.00) were prepared by one step sol-gel self-ignition approach. XRD and FESEM were used to examine the formation of a single-phase and variations in the grain size with the increasing contents of RE elements in Ni–Zn ferrite NPs. FTIR confirmed the vibrational studies of the RE doped spinel ferrite. The saturation magnetization, remanence, and coercivity elucidated...